Combinatorial Chemistry, Part B by Guillermo Morales, Barry A. Bunin

By Guillermo Morales, Barry A. Bunin

Combinatorial Chemistry encompasses either the layout of compounds for particular pharmacological use and the screening of molecules in excessive throughput computerized assessments to discover energetic brokers with particular services. *Analytical techniques*Direct sorting break up and pool combinatorial synthesis*Linkers and their applications*Microwave assisted synthesis*Oligosaccharide chemistry*Peptide Synthesis and Screening*Polymer assisted approaches*Small molecule and heterocycle synthesis

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A. Yurek, D. L. Branch, and M. Kuo, J. Comb. Chem. 4, 138 (2002). 20 E. W. Taylor, M. G. Qian, and G. D. Dollinger, Anal. Chem. 70, 3339 (1998). 5 0 100 200 300 400 500 600 700 800 900 m/z 1000 0 100 200 300 400 500 600 700 800 900 m/z 1000 13 Fig. 7. Mass spectra of LIB1-1 (A) and LIB1-2 (B) at sample cone voltage of 10, 20, 30, and 40 V. ) 14 analytical techniques [1] [100% relative abundance (RA)] and 2MHþ (dimer, 50% RA) can be found at 10 V for these compounds. Parent ions have been broken apart as the sample cone voltage increases from 10 to 40 V.

Kay, O. E. Lorthioir, N. J. Parr, M. Congreve, S. C. McKeown, J. J. Scicinski, and S. V. Ley, Biotechnol. Bioeng. 71, 110 (2001). [2] qualitative colorimetric tests for sps 23 Scheme 1. Amino acids were tested at all possible levels of protection. This enabled us to differentiate between test results caused by a given free functional group and results that may have been caused by other chemical moieties in the molecule. syringes fitted with polypropylene filter discs using standard solid-phase peptide synthesis procedures.

E. Lorthioir, N. J. Parr, M. Congreve, S. C. McKeown, J. J. Scicinski, and S. V. Ley, Biotechnol. Bioeng. 71, 110 (2001). [2] qualitative colorimetric tests for sps 23 Scheme 1. Amino acids were tested at all possible levels of protection. This enabled us to differentiate between test results caused by a given free functional group and results that may have been caused by other chemical moieties in the molecule. syringes fitted with polypropylene filter discs using standard solid-phase peptide synthesis procedures.

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